NWT BWR/Q-Chem Program
NWT developed the PWR/Q-Chem program in late 1984 to provide utilities with a method to
validate their analytical procedures and to assess their laboratory capabilities relative
to those of other utilities by analysis of blind samples. In mid-1987 NWT developed
BWR/Q-Chem to provide a similar service for BWRs. Both programs are supportive of the
objectives outlined for spiked samples in INPO Good Practices CY-701, "Chemistry
Quality Control Program," INPO 83-016, Rev. 2, August 1989, CY-702,
"Verification of Analytical Performance," INPO 83-107, Rev. 1, November 1985,
the laboratory performance guidelines and blind sample program in "Guidelines for
Chemistry at Nuclear Power Stations," INPO 88-021, Rev. 1, September 1991, and
"Guidelines for Chemistry at Nuclear Power Stations," INPO 88-021, Rev. 2,
October 1995.
BWR/Q-Chem sample matrices and concentration ranges are shown below. Sample sets are provided on a quarterly basis.
Each quarterly sample set consists of three 250 ml bottles containing identical mixtures
of chloride, sulfate, and silica at concentrations typical for reactor water. In addition,
two other species selected from the sample description table are provided as unknowns.
These additional samples also are provided in triplicate. A backup aliquot of each sample
is included in the original shipping container for return to NWT in the event concerns
arise relative to the effects of sample shipment. After sample analysis, each utility
summarizes its results and analysis techniques on a provided form and returns it to NWT.
Results can be submitted to NWT using the report form.
When the results have been received, a quarterly report is issued summarizing and
discussing utility results and the techniques employed for each analysis. Q-Chem
participants are identified by a letter in the report and the letter designation for each
laboratory is disclosed only in its report transmittal letter.
The cost of the basic NWT BWR/Q-Chem program is shown in the subscription form. Additional sample sets may also
be acquired.
NWT also has developed custom programs for several utilities. If the standard Q-Chem
program does not fulfill all of your needs, we will work with you to establish a more
responsive program. Please see the Custom Q-Chem Samples page.
Questions regarding the Q-Chem program should be directed to Mike Miller or Mary Hyde at
(408) 281-1100 or lab@nwtcorp.com.
Subscription Forms
| XRF Compatible
Filters |
Non-XRF Compatible Filters |
Print out and fax or mail to Mike Miller at NWT Corporation
(choose the Adobe® version or the web page version)
Adobe® Version
Web Page Version |
Print out and fax or mail to Mike Miller at NWT Corporation
(choose the Adobe® version or the web page version)
Adobe® Version
Web Page Version |
Adobe® Reader® is required to view and print the Adobe®
Versions of the BWR/Q-Chem Subscription Forms. Click here to
download Adobe® Reader® if you do not already have it installed on
your computer.
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Report Form
| BWR/Q-Chem Report Form |
Web reporting is not available at this time.
Please fax (408-578-0790) or e-mail your results.
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BWR/Q-Chem Sample
Description
| Species |
Matrix |
Concentration
Range |
Chloridea
Sulfatea
Silicaa
Boron
Nitrite
TOC
Sodium
Calcium
Magnesium
Sulfate
Chloride
Sodium Pentaborate |
Pure Water |
1 - 100 ppb
1-100 ppb
5 - 100 ppb
1 - 3000 ppm
200 - 1000 ppm
0.2 - 2.0 ppm
5 - 20000 ppb
25 - 100 ppm
2 - 10 ppm
20 - 250 ppm
5 - 50 ppm
10 - 15% |
Iron
Copper
Nickel
Chromium
Zinc |
Ion Exchange
Membrane |
0.002 - 1 mg/filter
0.04 - 2 mg/filter
0.01 - 1 mg/filter
0.02 - 0.5 mg/filter
0.02 - 1.5 mg/filter |
Iron
Copper
Nickel
Chromium
Zinc |
0.45 µm
Filterb |
0.04 - 10 mg/filter
0.02 - 1 mg/filter
0.01 - 1 mg/filter
0.01 - 0.25 mg/filter
0.01 - 0.7 mg/filter |
Iron
Copper
Nickel
Chromium
Zinc
Cobalt |
0.15% Nitric
Acidc |
1 - 100 ppm
0.2 - 20 ppm
0.1 - 10 ppm
0.1 - 5 ppm
0.1 - 20 ppm
1 - 100 ppb |
- Provided in Sample A each quarter.
- 0.45 µm filters are customarily radioactive. The total activity per filter is usually
less than one (1) µCi.
- Nitric acid matrix and elevated concentrations selected to simulate acid dissolution of
feedwater filters.
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